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Geochemical analysis of fine grained (<20 μm) tephra found in ice cores is inherently difficult, due to the typically low number and small size of available particles. Ice core tephra samples require specialized sample preparation techniques to maximize the amount of information that can be gained from these logistically limited samples that may provide important chronology to an ice record, as well as linking glacial, marine and terrestrial sediments. We have developed a flexible workflow for preparation of tephra and cryptotephra samples to allow accurate and robust geochemical fingerprinting, which is fundamental to tephrochronology. The samples can be prepared so that secondary electron imagery can be obtained for morphological characterization of the samples to ensure that the sample is tephra-bearing and then the sample can be further prepared for quantitative electron microprobe analysis using wavelength dispersive techniques (EMP-WDS), scanning electron microscopy with energy dispersive spectrometry (SEM-EDS), laser ablation inductively coupled mass spectrometry (LA-ICP-MS) or secondary ion mass spectrometry (SIMS). Some samples may be too small for typical instrumentation conditions to be used (i.e. 20 μm beam on the EMP) to analyze for geochemistry and we present other techniques that can be employed to obtain accurate, although less precise, geochemistry. Methods include analyzing unpolished tephra shards less than 5 μm in diameter with a 1 μm beam on an SEM; using the “broad beam overlap” EMP method on irregular particles less than 20 μm in diameter, and analyzing microlitic shards as well as aphyric shards using EMP to increase the number of analyzed shards in low abundance tephra layers. The methods presented are flexible enough to be employed in other geological environments (terrestrial, marine and glacial) which will help maximize and integrate multiple environments into the overall tephra framework. 相似文献
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当强震台站场地资料不完整时,所收集到的强震数据因缺乏准确的场地类别信息而难以有效利用。为解决这一问题,本文提出一种基于离散Fréchet距离的强震台站场地分类方法。将获取到的664个KiK-net台站场地按照《建筑抗震设计规范（GB 50011—2010）》进行分类,并构建2个数据集。利用数据集1得到Ⅰ、Ⅱ、Ⅲ类场地标准谱比曲线,并结合离散Fréchet距离对数据集2中的台站进行场地分类,统计分类成功率与误判率。统计结果表明,本文方法能较准确地对场地进行分类,且误判率在可接受范围内。将本文方法分类统计结果与斯皮尔曼秩相关系数法分类的成功率与误判率进行对比,结合本文方法分类后得到的平均谱比曲线,均可表明应用本文方法进行强震台站场地分类具有合理性。 相似文献
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Influence of IHSS Standard and Reference Materials on Copper and Mercury Toxicity to Vibrio fischeri
The reduction in light emission of the marine bacterium Vibrio fischeri used in the standard Microtox® bioassay was measured for the metals copper and mercury. The concentration at which the light emission was reduced by 50% (EC50) was determined to be (3.43 ± 0.83) μmol/L for Cu2+ and (0.66 ± 0.01) μmol/L for Hg2+. The reduction of the toxicity of these metals by humic and fulvic acids were studied using IHSS Standard and Reference Materials. Copper toxicity was reduced 17...20% by the soil and peat fulvic acids and 9...20% by the aquatic fulvic acids. While there appeared to be little difference in the reduction of Cu toxicity by fulvic acids from soils, peats, or aquatic systems, Hg toxicity was reduced 3.6...7.3% by the soils and peats, while aquatic fulvic acids reduced Hg toxicity 14...16%. Soil fulvic acids appear to have significantly less capacity to reduce Hg toxicity than Cu toxicity. Humic acids had much higher reductions of Cu toxicity (44...124%) compared to the fulvic acids, with little difference between aquatic and soil or peat humic acids, 44...124% and 67...100%, respectively. However, humic and fulvic acids, regardless of origin, had approximately the same effect on Hg toxicity with 3.5...16% reduction by fulvic acids and 8...20% reduction by humic acids. Unlike the fulvic acids, no clear trend was observed relative to origin of the humic acids. There was no correlation between percent reduction of Cu or Hg toxicity by the organic compounds and copper binding capacity (CuBC), C/N ratio, or carboxyl content of the materials. Examination of natural organic matter (NOM) isolated by reverse osmosis techniques from three water sources had reductions of both Cu and Hg toxicity that were most similar to the Suwannee River and Nordic fulvic acids. 相似文献
96.
U. Irmer 《洁净——土壤、空气、水》2000,28(1):7-14
The New EC Framework Water Directive: Assessment of the Chemical and Ecological Status of Surface Waters The main objective of the draft EC Framework Water Directive is the good quality of all surface waters. The directive provides for an assessment of the chemical status of surface waters (EU‐wide valid environmental quality standards for approximately 30 priority substances) and a five‐stage ecological classification of waters, comprising the stages high, good, moderate, poor, and bad. The starting point for the assessment are the reference conditions, which are defined as corresponding to high water quality and characterising a water status with no significant anthropogenic impact. The reference sites in the various water body types are to be selected using hydromorphological and physico‐chemical parameters and subsequently characterised by means of biological parameters. For surface waters, three groups of characteristics are provided for, namely: 1. with priority the biology – in the case of surface waters – with the four elements phytoplankton, macrophytes/phytobenthos, benthic invertebrate fauna, and fish fauna; 2. supporting the hydromorphology, e.g. flowing waters with the three elements hydrological regime, river continuity, and morphological conditions and 3. supporting the physico‐chemical conditions with the three elements general conditions, specific synthetic pollutants, and specific non synthetic pollutants (other than the priority substances of the chemical status). 相似文献
97.
标准贯入试验是现场测定土体工程性质的重要原位试验,是现场快速判定土体密实度的重要依据,具有及时、可靠、经济等特点,在地质勘察中被广泛的应用。本文通过介绍标准贯入试验的基本原理和设备,比较了英国规范、美国ASTM规范和我国岩土工程勘察规范之间标准贯入试验的差异,介绍了标准贯入试验所适用的经验公式,结合在美国ASTM规范指导下具体的工程实践结果,应用标准贯入试验的结果分析了苏丹国尼罗河Dagash流域内的土体工程性质,对比钻探所得土样和袖珍贯入测力计试验结果,验证了标贯结果的正确性。 相似文献
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Mary D. Curtis 《The Journal of geography》2019,118(3):130-142
Preparing learners for the future requires twenty-first-century teaching that integrates professional tools in the classroom. Geospatial technologies (GST), which represent geographical professional technologies, lack robust integration in high school geography. Researchers continue to ask why educators teach about rather than with GST. Understanding teacher decisions is paramount. This mixed methods study examined commonalities among teachers who use GST using Mishra and Koehler’s (2006) Technological, Pedagogical, Content Knowledge (TPCK) framework as a theoretical lens. This investigation examined whether geography teachers who exhibit stronger geospatial TPCK used GST more frequently than other teachers who exhibited a less developed knowledge base. 相似文献
100.